Structural characterization of Au nano bipyramids: Reshaping under thermal annealing, the capping agent effect and surface decoration with Pt

Maria Fernanda Torresan; Paula C. Angelomé; Lourdes Bazán-Diaz; J. Jesus Velázquez-Salazar; Rubén Mendoza-Cruz; Rodrigo A. Iglesias; Miguel José-Yacamán

doi:10.1088/1361-6528/ab0144

Structural characterization of Au nano bipyramids: Reshaping under thermal annealing, the capping agent effect and surface decoration with Pt

Maria Fernanda Torresan, Paula C. Angelomé, Lourdes Bazán-Diaz, J. Jesus Velázquez-Salazar, Rubén Mendoza-Cruz, Rodrigo A. Iglesias, Miguel José-Yacamán

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

Anisotropic gold nanoparticles offer potential applications due to their functionalities and shape-dependent properties. Reshaping noble metal nanoparticles is an interesting field with optical, surface-enhanced Raman spectroscopy, catalytic applications and potential application as a photothermic therapy. This work comprises a structural study on gold nano bipyramids (Au NBPs) and nanodumbbells, and the evolution of Au NBPs capped with cetyltrimethylammonium bromide and dodecanethiol through an in situ and ex situ heating process in high vacuum. Also, we study the reshaping of Au NBPs by the addition of Pt to study the surface modification and the strain generated on a single particle by geometric phase analysis.

Original language	English (US)
Article number	205701
Journal	Nanotechnology
Volume	30
Issue number	20
DOIs	https://doi.org/10.1088/1361-6528/ab0144
State	Published - Mar 5 2019
Externally published	Yes

Keywords

gold nano bipyramids
ligand exchange
Pt deposition
thermal annealing

ASJC Scopus subject areas

Bioengineering
Chemistry(all)
Materials Science(all)
Mechanics of Materials
Mechanical Engineering
Electrical and Electronic Engineering

Access to Document

10.1088/1361-6528/ab0144

Cite this

@article{32ba4ef894ad4e60b3ac4de866691b21,

title = "Structural characterization of Au nano bipyramids: Reshaping under thermal annealing, the capping agent effect and surface decoration with Pt",

abstract = "Anisotropic gold nanoparticles offer potential applications due to their functionalities and shape-dependent properties. Reshaping noble metal nanoparticles is an interesting field with optical, surface-enhanced Raman spectroscopy, catalytic applications and potential application as a photothermic therapy. This work comprises a structural study on gold nano bipyramids (Au NBPs) and nanodumbbells, and the evolution of Au NBPs capped with cetyltrimethylammonium bromide and dodecanethiol through an in situ and ex situ heating process in high vacuum. Also, we study the reshaping of Au NBPs by the addition of Pt to study the surface modification and the strain generated on a single particle by geometric phase analysis.",

keywords = "gold nano bipyramids, ligand exchange, Pt deposition, thermal annealing",

author = "Torresan, {Maria Fernanda} and Angelom{\'e}, {Paula C.} and Lourdes Baz{\'a}n-Diaz and Vel{\'a}zquez-Salazar, {J. Jesus} and Rub{\'e}n Mendoza-Cruz and Iglesias, {Rodrigo A.} and Miguel Jos{\'e}-Yacam{\'a}n",

note = "Funding Information: Mar�a Fernanda Torresan Paula C Angelom� Lourdes Baz�n-D�az J Jes�s Vel�zquez-Salazar Rub�n Mendoza-Cruz Rodrigo A Iglesias Miguel Jos�-Yacam�n Mar�a Fernanda Torresan Paula C Angelom� Lourdes Baz�n-D�az J Jes�s Vel�zquez-Salazar Rub�n Mendoza-Cruz Rodrigo A Iglesias Miguel Jos�-Yacam�n Instituto de Investigaciones en Fisicoqu�mica de C�rdoba, Universidad Nacional de C�rdoba, INFIQC CONICET, Departamento de Fisicoqu�mica, Facultad de Ciencias Qu�micas, Pabell�n Argentina, Ala 1 Piso 2, Ciudad Universitaria, C�rdoba 5000, Argentina Gerencia Qu�mica—Centro At�mico Constituyentes, Comisi�n Nacional de Energ�a, At�mica, CONICET, Av. Gral. Paz 1499, B1650KNA San Mart�n, Buenos Aires, Argentina Department of Biomedical Engineering, The University of Texas at San Antonio, One UTSA Circle, San Antonio, TX 78249, United States of America Department of Physics & Astronomy, The University of Texas at San Antonio, One UTSA Circle, San Antonio, TX 78249, United States of America Mar�a Fernanda Torresan, Paula C Angelom�, Lourdes Baz�n-D�az, J Jes�s Vel�zquez-Salazar, Rub�n Mendoza-Cruz, Rodrigo A Iglesias and Miguel Jos�-Yacam�n 2019-05-17 2019-03-05 13:11:54 cgi/release: Article released cgi/mmedia: Updated ToC/abstract link cgi/mmedia: Removed ToC/abstract link bin/incoming: New from .zip Fulbright Association https://doi.org/10.13039/100010629 Consejo Nacional de Investigaciones Cient�ficas y T�cnicas (CONACYT) https://doi.org/10.13039/501100002923 Consejo Nacional de Ciencia y Tecnolog�a (CONICET) https://doi.org/10.13039/501100003141 Welch Foundation https://doi.org/10.13039/100000928 The Welch Foundation supported this work through G yes Anisotropic gold nanoparticles offer potential applications due to their functionalities and shape-dependent properties. Reshaping noble metal nanoparticles is an interesting field with optical, surface-enhanced Raman spectroscopy, catalytic applications and potential application as a photothermic therapy. This work comprises a structural study on gold nano bipyramids (Au NBPs) and nanodumbbells, and the evolution of Au NBPs capped with cetyltrimethylammonium bromide and dodecanethiol through an in situ and ex situ heating process in high vacuum. Also, we study the reshaping of Au NBPs by the addition of Pt to study the surface modification and the strain generated on a single particle by geometric phase analysis. � 2019 IOP Publishing Ltd [1] Brust M and Kiely C J 2002 Colloids Surf. A Physicochem. Eng. Asp. 202 175 10.1016/S0927-7757(01)01087-1 Brust M and Kiely C J Colloids Surf. A Physicochem. Eng. Asp. 0927-7757 202 2002 175 [2] Cobley C M, Chen J, Cho E C, Wang L V and Xia Y 2011 Chem. Soc. Mater. 40 44 Cobley C M, Chen J, Cho E C, Wang L V and Xia Y Chem. Soc. 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year = "2019",

month = mar,

day = "5",

doi = "10.1088/1361-6528/ab0144",

language = "English (US)",

volume = "30",

journal = "Nanotechnology",

issn = "0957-4484",

publisher = "IOP Publishing Ltd.",

number = "20",

}

TY - JOUR

T1 - Structural characterization of Au nano bipyramids

T2 - Reshaping under thermal annealing, the capping agent effect and surface decoration with Pt

AU - Torresan, Maria Fernanda

AU - Angelomé, Paula C.

AU - Bazán-Diaz, Lourdes

AU - Velázquez-Salazar, J. Jesus

AU - Mendoza-Cruz, Rubén

AU - Iglesias, Rodrigo A.

AU - José-Yacamán, Miguel

N1 - Funding Information: Mar�a Fernanda Torresan Paula C Angelom� Lourdes Baz�n-D�az J Jes�s Vel�zquez-Salazar Rub�n Mendoza-Cruz Rodrigo A Iglesias Miguel Jos�-Yacam�n Mar�a Fernanda Torresan Paula C Angelom� Lourdes Baz�n-D�az J Jes�s Vel�zquez-Salazar Rub�n Mendoza-Cruz Rodrigo A Iglesias Miguel Jos�-Yacam�n Instituto de Investigaciones en Fisicoqu�mica de C�rdoba, Universidad Nacional de C�rdoba, INFIQC CONICET, Departamento de Fisicoqu�mica, Facultad de Ciencias Qu�micas, Pabell�n Argentina, Ala 1 Piso 2, Ciudad Universitaria, C�rdoba 5000, Argentina Gerencia Qu�mica—Centro At�mico Constituyentes, Comisi�n Nacional de Energ�a, At�mica, CONICET, Av. Gral. Paz 1499, B1650KNA San Mart�n, Buenos Aires, Argentina Department of Biomedical Engineering, The University of Texas at San Antonio, One UTSA Circle, San Antonio, TX 78249, United States of America Department of Physics & Astronomy, The University of Texas at San Antonio, One UTSA Circle, San Antonio, TX 78249, United States of America Mar�a Fernanda Torresan, Paula C Angelom�, Lourdes Baz�n-D�az, J Jes�s Vel�zquez-Salazar, Rub�n Mendoza-Cruz, Rodrigo A Iglesias and Miguel Jos�-Yacam�n 2019-05-17 2019-03-05 13:11:54 cgi/release: Article released cgi/mmedia: Updated ToC/abstract link cgi/mmedia: Removed ToC/abstract link bin/incoming: New from .zip Fulbright Association https://doi.org/10.13039/100010629 Consejo Nacional de Investigaciones Cient�ficas y T�cnicas (CONACYT) https://doi.org/10.13039/501100002923 Consejo Nacional de Ciencia y Tecnolog�a (CONICET) https://doi.org/10.13039/501100003141 Welch Foundation https://doi.org/10.13039/100000928 The Welch Foundation supported this work through G yes Anisotropic gold nanoparticles offer potential applications due to their functionalities and shape-dependent properties. Reshaping noble metal nanoparticles is an interesting field with optical, surface-enhanced Raman spectroscopy, catalytic applications and potential application as a photothermic therapy. This work comprises a structural study on gold nano bipyramids (Au NBPs) and nanodumbbells, and the evolution of Au NBPs capped with cetyltrimethylammonium bromide and dodecanethiol through an in situ and ex situ heating process in high vacuum. Also, we study the reshaping of Au NBPs by the addition of Pt to study the surface modification and the strain generated on a single particle by geometric phase analysis. � 2019 IOP Publishing Ltd [1] Brust M and Kiely C J 2002 Colloids Surf. A Physicochem. Eng. Asp. 202 175 10.1016/S0927-7757(01)01087-1 Brust M and Kiely C J Colloids Surf. A Physicochem. Eng. Asp. 0927-7757 202 2002 175 [2] Cobley C M, Chen J, Cho E C, Wang L V and Xia Y 2011 Chem. Soc. Mater. 40 44 Cobley C M, Chen J, Cho E C, Wang L V and Xia Y Chem. Soc. 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PY - 2019/3/5

Y1 - 2019/3/5

N2 - Anisotropic gold nanoparticles offer potential applications due to their functionalities and shape-dependent properties. Reshaping noble metal nanoparticles is an interesting field with optical, surface-enhanced Raman spectroscopy, catalytic applications and potential application as a photothermic therapy. This work comprises a structural study on gold nano bipyramids (Au NBPs) and nanodumbbells, and the evolution of Au NBPs capped with cetyltrimethylammonium bromide and dodecanethiol through an in situ and ex situ heating process in high vacuum. Also, we study the reshaping of Au NBPs by the addition of Pt to study the surface modification and the strain generated on a single particle by geometric phase analysis.

AB - Anisotropic gold nanoparticles offer potential applications due to their functionalities and shape-dependent properties. Reshaping noble metal nanoparticles is an interesting field with optical, surface-enhanced Raman spectroscopy, catalytic applications and potential application as a photothermic therapy. This work comprises a structural study on gold nano bipyramids (Au NBPs) and nanodumbbells, and the evolution of Au NBPs capped with cetyltrimethylammonium bromide and dodecanethiol through an in situ and ex situ heating process in high vacuum. Also, we study the reshaping of Au NBPs by the addition of Pt to study the surface modification and the strain generated on a single particle by geometric phase analysis.

KW - gold nano bipyramids

KW - ligand exchange

KW - Pt deposition

KW - thermal annealing

UR - http://www.scopus.com/inward/record.url?scp=85062884441&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=85062884441&partnerID=8YFLogxK

U2 - 10.1088/1361-6528/ab0144

DO - 10.1088/1361-6528/ab0144

M3 - Article

C2 - 30673656

AN - SCOPUS:85062884441

SN - 0957-4484

VL - 30

JO - Nanotechnology

JF - Nanotechnology

IS - 20

M1 - 205701

ER -

Structural characterization of Au nano bipyramids: Reshaping under thermal annealing, the capping agent effect and surface decoration with Pt

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