Raman spectroscopic characterization of graphites: A re-evaluation of spectra/ structure correlation

Leszek Nikiel; Paul W. Jagodzinski

doi:10.1016/0008-6223(93)90091-N

Raman spectroscopic characterization of graphites: A re-evaluation of spectra/ structure correlation

Leszek Nikiel
, Paul W. Jagodzinski

Research output: Contribution to journal › Article › peer-review

187 Scopus citations

Abstract

First-order Raman scattering from nuclear grade graphites, highly oriented pyrolytic graphite (HOPG) and grafoil are reported. Spectral parameters such as band positions and bandwidths and their correlations with domain size values are presented. The dependence between the intensity ratio of the Raman D and G bands and the domain size L_a show inversely proportional behavior. However, the slope of the line fitted to the experimental points is different from previously reported results.

Original language	English (US)
Pages (from-to)	1313-1317
Number of pages	5
Journal	Carbon
Volume	31
Issue number	8
DOIs	https://doi.org/10.1016/0008-6223(93)90091-N
State	Published - 1993
Externally published	Yes

Keywords

Raman spectroscopy
graphite

ASJC Scopus subject areas

General Chemistry
General Materials Science

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10.1016/0008-6223(93)90091-N

Cite this

@article{2f1e995ec70e41ae869b415c7f4e96d5,

title = "Raman spectroscopic characterization of graphites: A re-evaluation of spectra/ structure correlation",

abstract = "First-order Raman scattering from nuclear grade graphites, highly oriented pyrolytic graphite (HOPG) and grafoil are reported. Spectral parameters such as band positions and bandwidths and their correlations with domain size values are presented. The dependence between the intensity ratio of the Raman D and G bands and the domain size La show inversely proportional behavior. However, the slope of the line fitted to the experimental points is different from previously reported results.",

keywords = "Raman spectroscopy, graphite",

author = "Leszek Nikiel and Jagodzinski, \{Paul W.\}",

note = "Funding Information: Ackno\&dgements-The authorsw ould like to thankD r. A. Pavlovic and Dr. M. Seehra for fruitful discussions and for providing X-ray datap rior to publication.S pecial thanksa re extendedt o Drs. J. Zondlo, P. Stansberry.a nd E. L. Fuller, Jr., for providingt he samplesu sed in these studies. This work was supportedb y the United States Departmento f Energy Grant No. DE-FGO2-91NPOOI59. Funding Information: a Domain sizes, L,, takenf rom ref.[l7]. b Data received from M. S. Seehra and A. S. Pavlovic ({\textquoteleft}Coal Based Nuclear Graphitesf or the New Production Gas Cooled Reactor{\textquoteright}, DOE Technical Report, Grant No. DE-FG02-91NPO0159). c Calculatedd ata.",

year = "1993",

doi = "10.1016/0008-6223(93)90091-N",

language = "English (US)",

volume = "31",

pages = "1313--1317",

journal = "Carbon",

issn = "0008-6223",

publisher = "Elsevier Ltd",

number = "8",

}

TY - JOUR

T1 - Raman spectroscopic characterization of graphites

T2 - A re-evaluation of spectra/ structure correlation

AU - Nikiel, Leszek

AU - Jagodzinski, Paul W.

N1 - Funding Information: Ackno&dgements-The authorsw ould like to thankD r. A. Pavlovic and Dr. M. Seehra for fruitful discussions and for providing X-ray datap rior to publication.S pecial thanksa re extendedt o Drs. J. Zondlo, P. Stansberry.a nd E. L. Fuller, Jr., for providingt he samplesu sed in these studies. This work was supportedb y the United States Departmento f Energy Grant No. DE-FGO2-91NPOOI59. Funding Information: a Domain sizes, L,, takenf rom ref.[l7]. b Data received from M. S. Seehra and A. S. Pavlovic (‘Coal Based Nuclear Graphitesf or the New Production Gas Cooled Reactor’, DOE Technical Report, Grant No. DE-FG02-91NPO0159). c Calculatedd ata.

PY - 1993

Y1 - 1993

N2 - First-order Raman scattering from nuclear grade graphites, highly oriented pyrolytic graphite (HOPG) and grafoil are reported. Spectral parameters such as band positions and bandwidths and their correlations with domain size values are presented. The dependence between the intensity ratio of the Raman D and G bands and the domain size La show inversely proportional behavior. However, the slope of the line fitted to the experimental points is different from previously reported results.

AB - First-order Raman scattering from nuclear grade graphites, highly oriented pyrolytic graphite (HOPG) and grafoil are reported. Spectral parameters such as band positions and bandwidths and their correlations with domain size values are presented. The dependence between the intensity ratio of the Raman D and G bands and the domain size La show inversely proportional behavior. However, the slope of the line fitted to the experimental points is different from previously reported results.

KW - Raman spectroscopy

KW - graphite

UR - https://www.scopus.com/pages/publications/0027806878

UR - https://www.scopus.com/pages/publications/0027806878#tab=citedBy

U2 - 10.1016/0008-6223(93)90091-N

DO - 10.1016/0008-6223(93)90091-N

M3 - Article

AN - SCOPUS:0027806878

SN - 0008-6223

VL - 31

SP - 1313

EP - 1317

JO - Carbon

JF - Carbon

IS - 8

ER -

Raman spectroscopic characterization of graphites: A re-evaluation of spectra/ structure correlation

Abstract

Keywords

ASJC Scopus subject areas

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